• Article dans une revue

Complementarity of Density Functional Theory and Nuclear Magnetic Resonance Tools To Probe the Nano-Layered Silicates Surface Chemistry and Morphology

Mathilde Poirier, Yannick Millot, Elisa Silva Gomes, Maguy Jaber, Virginie Herledan, Guillaume Laugel, Pierre Micoud, François Martin, Hélène Lauron-Pernot, Hervé Toulhoat

By combining experimental, spectroscopic, structural, and physical characterizations and extensive density functional theory simulations, unprecedented insight is gained on the local surface properties of synthetic talc nanoparticles, their structure, morphology and particle size distribution.…

Journal of Physical Chemistry C, 2020, 124 (1), pp.267-286. ⟨10.1021/acs.jpcc.9b05903⟩. ⟨hal-02457727⟩

• Communication dans un congrès

Direct insight into the activation mechanism of Fe and Sb catalysts by operando TEM and XAS techniques

Aliou Sadia Traore, Walid Baaziz, Zhou Yong, Andrei Khodakov, Mirella Virginie, E. Marceau, Vitaly Ordomsky, Sharmin Sharna, Valérie Briois, Ovidiu Ersen

20th International Microscopy Congress, Sep 2023, Busan (Corée), South Korea. ⟨hal-04523342⟩

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Cobalt-containing BEA zeolite for catalytic combustion of toluene

Anna Rokicińska, Marek Drozdek, Barbara Dudek, Barbara Gil, Piotr Michorczyk, Dalil Brouri, Stanislaw Dzwigaj, Piotr Kuśtrowski

Co-containing HAlBEA zeolite was obtained by conventional wet impregnation of HAlBEA zeolite with an aqueous Co(NO3)2.6 H2O solution, whereas Co-containing SiBEA zeolites were prepared by a two-step post-synthesis method. This approach consists of, in the first step, dealumination of parent BEA…

Applied Catalysis B: Environmental, 2017, 212, pp.59 - 67. ⟨10.1016/j.apcatb.2017.04.067⟩. ⟨hal-01517429⟩

• Thèse

Investigation of the plate-impact method as a precursor of physical phenomena and chemical processes, L'étude de la méthode de l'impact par plaque comme précurseur des phénomènes physiques et des processus chimiques

Maya Mounir Daou

This manuscript aims at characterizing a new device based on a plate impact on a liquid surface to generate cavitation and evaluate its potential to induce chemical reactions. The device is composed of a reactor containing a liquid that a piston hits due to pressure difference. This impact…, Ce manuscrit a pour but d'étudier un nouveau dispositif générateur de cavitation dont le potentiel favorable à l'intensification de réactions chimiques est évalué. Ce dispositif est constitué d'une plaque mobile qui frappe un liquide contenu dans un réacteur. L'impact génère une…

Chemical and Process Engineering. Université Pierre et Marie Curie - Paris VI, 2017. English. ⟨NNT : 2017PA066245⟩. ⟨tel-01692697v2⟩

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Experimental evidence of NO SCR mechanism in the presence of the BEA zeolite with framework and extra-framework cobalt species

Paweł Boroń, Lucjan Chmielarz, Barbara Gil, Bartosz Marszałek, Stanislaw Dzwigaj

Temperature-programmed desorption (TPD), temperature-programmed surface reaction (TPSR) and stop flow-TPD techniques as well as FT-IR spectroscopy of pre-adsorbed NH3 and NO are applied to characterize active sites present in Co-containing BEA zeolites. Cobalt is introduced into BEA zeolite by…

Applied Catalysis B: Environmental, 2016, 198, pp.457-470. ⟨10.1016/j.apcatb.2016.06.012⟩. ⟨hal-01329568⟩

• Article dans une revue

Platinum-zeolite hybrid catalyst for the electrooxidation of formic acid

Lu Zhang, Juan V Perales-Rondón, Angélica Thomère, Juliette Blanchard, Carlos M Sánchez-Sánchez

Formic acid oxidation reaction (FAOR) was studied using different platinum-zeolites hybrid catalysts. The catalysts were prepared by addition of two different forms of the ZSM-5 zeolite (ZSM-5-H+ and ZSM-5-NH4+) to an ink containing Vulcan carbon support and Pt nanoparticles (NPs). TEM images…

Journal of Electroanalytical Chemistry, 2021, 896, pp.115491. ⟨10.1016/j.jelechem.2021.115491⟩. ⟨hal-03274842v2⟩

• Article dans une revue

Antibacterial activity of intermetallic NixMgy and NiO–MgO phases in nickel-magnesium oxide nanocomposites

N. Ouafek, N. Keghouche, Patricia Beaunier, Jacqueline Belloni, Mehran Mostafavi

Radiation Physics and Chemistry, 2023, 202, pp.110499. ⟨10.1016/j.radphyschem.2022.110499⟩. ⟨hal-04310742⟩

• Article dans une revue

A Rotaxane Scaffold Bearing Multiple Redox Centers: Synthesis, Surface Modification and Electrochemical Properties

Marie Steffenhagen, Alina Latus, Thi Minh Nguyet Trinh, Iwona Nierengarten, Ivan T. Lucas, Suzanne Joiret, Jessem Landoulsi, Béatrice Delavaux-Nicot, Jean-François Nierengarten, Emmanuel Maisonhaute

A rotaxane scaffold incorporating two dithiolane anchoring units for the modification of gold surfaces has been functionalized with multiple copies of a redox unit, namely ferrocene. Surface modification has been first assessed at the single molecule level by atomic force microscopy (AFM) and…

Chemistry - A European Journal, 2018, 24 (7), pp.1701-1708. ⟨10.1002/chem.201705245⟩. ⟨hal-01722802⟩

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Controlled preparation of CoPdSiBEA zeolite catalysts for selective catalytic reduction of NO with methane and their characterisation by XRD, DR UV-vis, TPR, XPS

Ana Rodrigues, Patrick da Costa, C. Methivier, S. Dzwigaj

The Pd0.15SiBEA and CoxPd0.15SiBEA zeolites (where x= 1.0 and 3.0 wt.% Co) are prepared by a two-step postsynthesis method which allows to control the introduction of palladium and cobalt into zeolite and thus to obtain catalysts with specific bimetallic Pd and Co sites. The effect of Co content on…

Catalysis Today, 2011, 176, pp.72-76. ⟨10.1016/j.cattod.2011.03.013⟩. ⟨hal-00666188⟩

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Physico-chemical properties of FeAlBEA and FeSiBEA zeolites and their catalytic activity in the SCR of NO with ethanol or methane

Janusz Janas, Stanislaw Dzwigaj

FeAlBEA and FeSiBEA zeolites are prepared by a conventional ion exchange and a two-step postsynthesis method, respectively. Their physico-chemical properties are investigated by XRD, FTIR, and diffuse reflectance UV-vis. For FeAlBEA zeolite, framework tetrahedral Fe(III), extra-framework octahedral…

Catalysis Today, 2011, 176 (1), pp.272-276. ⟨10.1016/j.cattod.2010.12.012⟩. ⟨hal-00666884⟩