• Article dans une revue

Surface plasmon resonance biosensors incorporating gold nanoparticles.

Erin Bedford, Jolanda Spadavecchia, Claire-Marie Pradier, Frank Gu

SPR biosensing is increasingly popular for the detection of a multitude of biomolecules. It offers label-free detection and study of proteins, nucleic acids, and other biomolecules in real time. A recent trend involves incorporation of AuNPs, either within the sensing surface itself or as signal…

Macromolecular Bioscience, 2012, 12, pp.724-739. ⟨10.1002/mabi.201100435⟩. ⟨hal-00745836⟩

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Selective catalytic reduction of NO on single site FeSiBEA zeolite catalyst: Influence of the C1 and C2 reducing agents on the catalytic properties

Janusz Janas, Wojciech Rojek, Tetsuya Shishido, Stanislaw Dzwigaj

FeSiBEA zeolite with 0.8 Fe wt% is prepared in acidic condition (pH 2.5) by a two-step postsynthesis method which allows to incorporate iron into framework of zeolite as mononuclear distorted tetrahedral Fe(III) species, as evidenced by XRD, diffuse reflectance UV-vis and X-ray absorption…

Applied Catalysis B: Environmental, 2012, 123-124, pp.134-140. ⟨10.1016/j.apcatb.2012.04.026⟩. ⟨hal-00744653⟩

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Bioconjugated gold nanorods to enhance the sensitivity of FT-SPR-based biosensors

Jolanda Spadavecchia, Sandra Casale, Souhir Boujday, Claire-Marie Pradier

n this paper, we report a feasible solvent-free approach for the synthesis and self-assembling of gold nanorods after bioconjugation to antibodies; scanning electron microscopy (SEM) and transmission electron microscopy (TEM) images revealed a remarkable shape and size narrow distribution, as well…

Colloids and Surfaces B: Biointerfaces, 2012, 100, pp.1-8. ⟨10.1016/j.colsurfb.2012.03.035⟩. ⟨hal-00744490⟩

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Controlling the reproducibility of Coulomb blockade phenomena for gold nanoparticles on an organic monolayer/silicon system

L Caillard, S Sattayaporn, A-F Lamic-Humblot, S Casale, P Campbell, y J Chabal, Olivier Pluchery

Two types of highly ordered organic layers were prepared on silicon modified with an amine termination for binding gold nanoparticles (AuNPs). These two grafted organic monolayers (GOMs), consisting of alkyl chains with seven or 11 carbon atoms, were grafted on oxide-free Si(111) surfaces as tunnel…

Nanotechnology, 2015, 26 (6), pp.065301. ⟨10.1088/0957-4484/26/6/065301⟩. ⟨hal-01114456⟩

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The Synthesis of Different Series of Cobalt BEA Zeolite Catalysts by Post-Synthesis Methods and Their Characterization

Renata Sadek, Karolina Chalupka-Spiewak, Jean-Marc Krafft, Yannick Millot, Laetitia Valentin, Sandra Casale, Jacek Gurgul, Stanislaw Dzwigaj

Three series of zeolite catalysts Co all-silica and Co Al-containing zeolites beta were prepared for use in the selective oxidative dehydrogenation of propane to propylene. Two series of zeolite catalysts Co all-silica were prepared by a two-step postsynthesis method at pH = 2.5 and pH = 3.0-9.0,…

Catalysts, 2022, 12 (12), pp.1644. ⟨10.3390/catal12121644⟩. ⟨hal-04030832⟩

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Modelling of a Lean NOx-Trap system with NO/NO2 differentiation and sulfur poisoning

Alexis Manigrasso, Pierre Darcy, Patrick da Costa

One of the challenges in the automotive industry is to develop new vehicles and new technologies with minimal costs. In this context, modeling becomes an important tool for the design of future technologies by reducing the number of tests needed to develop a new exhaust system. With the emergence…

SAE International Journal of Fuels and Lubricants, 2010, 3 (2), pp.414-424. ⟨hal-00604776⟩

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The controlled synthesis of metal-acid bifunctional catalysts: Selective Pt deposition and nanoparticle synthesis on amorphous aluminosilicates

Jadid E. Samad, Juliette Blanchard, Celine Sayag, Catherine Louis, John R. Regalbuto

The rational synthesis of metal-acid bifunctional catalysts based on aluminosilicates will involve control over which domain – alumina or silica – the metal can be deposited on, as well as the control of particle size. These factors determine the ratio and proximity of the metal and acid sites. The…

Journal of Catalysis, 2016, 342, pp.213 - 225. ⟨10.1016/j.jcat.2016.08.002⟩. ⟨hal-01564217⟩

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Enhanced selectivity of 3-D ordered macroporous Pt/Al2O3 catalysts in nitrites removal from water

A.C. Sunil Sekhar, A. Zaki, S. Troncea, S. Casale, C.P. Vinod, J.P. Dacquin, P. Granger

Tailored macroporous mesoporous alumina supports have been successfully prepared using a single hard templating approach. Pt nanoparticles, showing similar physico-chemical properties, were homogeneously dispersed throughout the different alumina frameworks as catalytic active phase for drinking…

Applied Catalysis A : General, 2018, 564, pp.26-32. ⟨10.1016/j.apcata.2018.07.014⟩. ⟨hal-03984216⟩

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Identification and Location of Iron Species in Fe/SBA-15 Catalysts: Interest for Catalytic Fenton Reactions

Cécile Cornu, Jean-Luc Bonardet, Sandra Casale, Anne Davidson, Sebastien Abramson, Gilles André, Florence Porchet, Ivana Grcic, Vesna Tomasic, Dinko Vujevic

We have used a single SBA-15 silica batch (mesopore diameter of 7.1 nm) and the two-solvent impregnation technique with either pentane or cyclohexane to prepare model samples in which an initial aqueous solution of salt precursor (iron nitrate or iron chloride) is deposited mainly inside silica…

Journal of Physical Chemistry C, 2011, 116, pp.3437-3448. ⟨10.1021/jp2038625⟩. ⟨hal-00688081⟩

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Micelle formation in ethyl-ammonium nitrate (an ionic liquid)

Sergio Bordel Velasco, Mireille Turmine, Dung Di Caprio, Pierre Letellier

Colloids and Surfaces A: Physicochemical and Engineering Aspects, 2006, 275 (1-3), pp.50-54. ⟨10.1016/j.colsurfa.2005.09.017⟩. ⟨hal-02354834⟩